Product Overview
This product is a general-purpose Zirconium Oxide (ZrO₂) Ceramic
Jar used for grinding and mixing materials in a planetary ball
mill. It consists of the main jar body and a sealing lid, forming a
complete containment system for high-energy milling processes. It
is a workhorse container in many labs for applications where high
purity and wear resistance are required.
Detailed Breakdown of Components & Materials
1. The Jar & Lid: Zirconium Oxide (Zirconia) Ceramic
Material Composition: The jar is made from Zirconium Oxide (ZrO₂),
a type of advanced technical ceramic. It is crucial to note that
most high-quality milling jars are actually Yttria-Stabilized
Zirconia (YSZ), meaning a small percentage of Yttrium Oxide is
added to the zirconia.
Why Stabilization? Pure zirconia undergoes a destructive crystal
phase change during heating and cooling. The yttria stabilizer
locks the zirconia in a tough, stable phase, preventing it from
cracking and giving it exceptional fracture resistance.
Key Material Properties:
- Extreme Hardness: Zirconia is very hard (over 9 on the Mohs scale),
making it highly resistant to abrasion from the grinding balls and
the sample material. This ensures a long lifespan.
- High Wear Resistance: It wears down very slowly, which minimizes
contamination of the sample from the jar itself.
- High Density (~6.0 g/cm³): The dense material increases the impact
energy of the grinding balls, leading to more efficient milling and
shorter processing times.
- Excellent Chemical Inertness: Zirconia is highly resistant to
corrosion from acids, alkalis, and various solvents, making it
suitable for both dry and wet milling.
- Low Contamination: The combination of low wear rate and chemical
inertness makes it the preferred choice for applications where
sample purity is critical (e.g., electronics, pharmaceuticals).
2. The Sealing System
The Lid: Typically made from the same zirconia material or a
robust, compatible material like PTFE or POM to ensure a good seal.
The Gasket/O-Ring: The lid incorporates a rubber O-ring (often made
of Viton or NBR for chemical resistance) that creates a secure,
leak-proof seal. This is essential for:
- Containing fine dust during dry milling.
- Preventing spillage of solvents and slurries during wet milling.
- Allowing the jar to be filled with an inert gas (like Argon) to
prevent oxidation of sensitive materials during milling.
Typical Applications
This type of jar is used across a wide range of scientific and
industrial fields for:
- Size Reduction: Grinding materials down to nano-sized powders.
- Mechanical Alloying: Combining metals into alloyed powders through
high-energy impacts.
- Mixing & Homogenization: Blending different powders into a
perfectly uniform mixture.
- Mechanochemistry: Inducing chemical reactions through mechanical
energy.
Specific Industries:
- Materials Science: Producing nanocomposites, amorphous alloys, and
advanced ceramics.
- Electronics: Synthesizing powders for capacitors, varistors, and
battery materials (e.g., cathode powders).
- Pharmaceuticals: Reducing particle size of active ingredients to
enhance bioavailability.
- Geology: Pulverizing rock and mineral samples for accurate chemical
analysis (XRF, XRD).
Critical Considerations Before Use
- Grinding Balls (Media): You MUST use grinding balls made of the
same material (Zirconia). Using a harder media (like tungsten
carbide) will rapidly damage and contaminate the jar. The size and
quantity of the balls are critical for efficient milling.
- Planetary Mill Compatibility: This jar is specifically designed for
planetary ball mills. You must ensure the jar's outer dimensions
and volume are compatible with the mounting clamps and the maximum
capacity of your specific mill model (e.g., Retsch, Fritsch, MTI,
etc.).
- Filling Ratio: For effective operation, the jar should never be
filled more than one-third to one-half of its total volume with a
combination of grinding balls and material. Overfilling prevents
the cascading motion required for effective grinding.
- Capacity: These jars come in various standard sizes (e.g., 50ml,
100ml, 250ml, 500ml, 1L). The choice depends on your required batch
size and mill compatibility.
Summary
The Zirconium Oxide Ceramic Ball Milling Tank is a premium,
durable, and versatile container for high-energy planetary ball
milling. Its primary advantages are its exceptional wear resistance
and low contamination profile, which are essential for achieving
pure, finely ground, and homogeneously mixed materials in research
and development laboratories. When paired with the correct zirconia
grinding balls and used in a compatible mill, it is a reliable and
critical tool for advanced material processing.